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How to properly use jacketed glass reactor?

Technical Knowledge 2014-05-12 09:47:22
The jacketed glass reactor is designed as jacketed glass, and the inner layer is placed in the reaction medium for stirring reaction, and the interlayer can be heated or cooled by using different cold and heat sources (refrigerant, hot water or hot oil). Under constant temperature conditions.

The jacketed glass reactor can be stirred under normal pressure or negative pressure according to the requirements of use, and can be used for reflux and distillation of the reaction solution. The jacketed glass reactor is a modern fine chemical plant. Ideal pilot and production equipment for biopharmaceutical and new material synthesis.

Jacketed glass reactor, please be familiar with the contents of the full-mode temperature machine part of this manual before installation, use, maintenance, inspection, etc.; the double-wall glass reactor power supply voltage must be consistent with the requirements of the instrument; The layer glass reactor is not suitable for high speed operation at no load; the life of the jacketed glass reactor electrical box has a great influence on the ambient temperature and humidity.

Please insist on speed regulation and motor drying; jacketed glass reactor first install the machine and then be wired by professional electrician, energize, ground terminal must be grounded.

The high temperature bath must be connected to the open switch; the jacketed glass reactor will be powered off within 5 minutes due to the inverter or capacitor discharge; the jacketed glass reactor should pay attention to the hard object (watch, ring, belt) Buckle, etc.) damage to the glass; double-glazed reactor must be carefully connected when connecting the vacuum tube to avoid excessive damage to the human body caused by the glass; jacketed glass reactor requires high-temperature circulating oil bath, pay attention to For high temperature damage to the human body, it is recommended to use a heat-conducting oil (dimethicone) with a kinematic viscosity of 100 as a solvent.

In particular, when paying attention to high-temperature circulation, the circulating pump should be turned on first to allow the heat-conductive solvent to circulate, and then slowly heat up.

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